Production and characterization of shape memory epoxy foam by an advances aqueous method
Shape memory foam is consider as an advantageous invention that has being gained researcher’s focus recently. The ability of shape memory foam is it will deform under certain mechanical forces and slowly recover back into its original shape as if it memories. This research suggested an advanced aqu...
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my-unimap-727022022-11-17T01:55:48Z Production and characterization of shape memory epoxy foam by an advances aqueous method Du Ngoc, Uy Lan, Dr. Shape memory foam is consider as an advantageous invention that has being gained researcher’s focus recently. The ability of shape memory foam is it will deform under certain mechanical forces and slowly recover back into its original shape as if it memories. This research suggested an advanced aqueous method to produce epoxy shape memory foam. This method is environmentally friendly because it is free from solvent. First of all, mixture of epoxy, polyamide, sodium bicarbonate and filler was prepared by using over-head stirrer. Next, the mixture was emulsified with distilled water using high stirring speed (1200 rpm – 2 minutes), following by addition of ammonium chloride solution into the mixture and stirred at 600 rpm for 2 minutes. Finally, the epoxy emulsion was casted into PP mould and cured. The uses of polyamide-epoxy adduct as the reversed ratio of polyamide and epoxy was explored to produce flexible epoxy. Due to polyamide derive from dimerize tall oil fatty acids (TOFAS), the polyamide-epoxy adduct was able to be emulsified at high speed stirring and without using emulsifier. It resulted in an epoxy emulsion similar to water/oil/water (W/O/W) system. Which, water worked as the continuous phase in emulsion system and also presented as the dispersed phase in epoxy resin. In addition, eggshell was used as an eco-green filler, which consisted of 95% by weight of calcium carbonate (CaCO3). Universiti Malaysia Perlis (UniMAP) Thesis en http://dspace.unimap.edu.my:80/xmlui/handle/123456789/72702 http://dspace.unimap.edu.my:80/xmlui/bitstream/123456789/72702/3/license.txt 8a4605be74aa9ea9d79846c1fba20a33 http://dspace.unimap.edu.my:80/xmlui/bitstream/123456789/72702/1/Page%201-24.pdf 110b5ce546feba459a1630fde6d675da http://dspace.unimap.edu.my:80/xmlui/bitstream/123456789/72702/2/Full%20text.pdf cbd7d66a0df6da43d0a05150c32fdbf3 http://dspace.unimap.edu.my:80/xmlui/bitstream/123456789/72702/4/Muhammad%20Syazwan.pdf b456f8489b8c50a2fa5659174cce6db3 Universiti Malaysia Perlis (UniMAP) Epoxy resins Porous materials Foamed materials Shape memory foam Polymer foam School of Materials Engineering |
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Universiti Malaysia Perlis |
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UniMAP Institutional Repository |
language |
English |
advisor |
Du Ngoc, Uy Lan, Dr. |
topic |
Epoxy resins Porous materials Foamed materials Shape memory foam Polymer foam |
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Epoxy resins Porous materials Foamed materials Shape memory foam Polymer foam Production and characterization of shape memory epoxy foam by an advances aqueous method |
description |
Shape memory foam is consider as an advantageous invention that has being gained researcher’s focus recently. The ability of shape memory foam is it will deform under certain mechanical forces and slowly recover back into its original shape as if it
memories. This research suggested an advanced aqueous method to produce epoxy shape memory foam. This method is environmentally friendly because it is free from solvent. First of all, mixture of epoxy, polyamide, sodium bicarbonate and filler was
prepared by using over-head stirrer. Next, the mixture was emulsified with distilled water using high stirring speed (1200 rpm – 2 minutes), following by addition of ammonium chloride solution into the mixture and stirred at 600 rpm for 2 minutes.
Finally, the epoxy emulsion was casted into PP mould and cured. The uses of polyamide-epoxy adduct as the reversed ratio of polyamide and epoxy was explored to produce flexible epoxy. Due to polyamide derive from dimerize tall oil fatty acids
(TOFAS), the polyamide-epoxy adduct was able to be emulsified at high speed stirring and without using emulsifier. It resulted in an epoxy emulsion similar to water/oil/water (W/O/W) system. Which, water worked as the continuous phase in emulsion system and also presented as the dispersed phase in epoxy resin. In addition, eggshell was used as an eco-green filler, which consisted of 95% by weight of calcium carbonate (CaCO3). |
format |
Thesis |
title |
Production and characterization of shape memory epoxy foam by an advances aqueous method |
title_short |
Production and characterization of shape memory epoxy foam by an advances aqueous method |
title_full |
Production and characterization of shape memory epoxy foam by an advances aqueous method |
title_fullStr |
Production and characterization of shape memory epoxy foam by an advances aqueous method |
title_full_unstemmed |
Production and characterization of shape memory epoxy foam by an advances aqueous method |
title_sort |
production and characterization of shape memory epoxy foam by an advances aqueous method |
granting_institution |
Universiti Malaysia Perlis (UniMAP) |
granting_department |
School of Materials Engineering |
url |
http://dspace.unimap.edu.my:80/xmlui/bitstream/123456789/72702/1/Page%201-24.pdf http://dspace.unimap.edu.my:80/xmlui/bitstream/123456789/72702/2/Full%20text.pdf http://dspace.unimap.edu.my:80/xmlui/bitstream/123456789/72702/4/Muhammad%20Syazwan.pdf |
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