Extraction Of Oil From Calophyllum Inophyllum Seeds Optimization And Kinetics Studies Of Ultrasonic-Assisted Extraction

Calophyllum inophyllum seeds oil was extracted using two different extraction techniques, namely, ultrasonic-assisted extraction (UAE) and Soxhlet extraction (SE). The highest oil yield attained from UAE was 55.44 ± 0.53 % at an extraction time of 20 min, extraction temperature 40 °C, ultrasonic pow...

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Main Author: Fuad, Faiznur Mohd
Format: Thesis
Language:English
Published: 2016
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Online Access:http://eprints.usm.my/45771/1/Extraction%20Of%20Oil%20From%20Calophyllum%20Inophyllum%20Seeds%20Optimization%20And%20Kinetics%20Studies%20Of%20Ultrasonic-Assisted%20Extraction.pdf
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spelling my-usm-ep.457712020-10-22T03:03:18Z Extraction Of Oil From Calophyllum Inophyllum Seeds Optimization And Kinetics Studies Of Ultrasonic-Assisted Extraction 2016-03 Fuad, Faiznur Mohd T Technology TP155-156 Chemical engineering Calophyllum inophyllum seeds oil was extracted using two different extraction techniques, namely, ultrasonic-assisted extraction (UAE) and Soxhlet extraction (SE). The highest oil yield attained from UAE was 55.44 ± 0.53 % at an extraction time of 20 min, extraction temperature 40 °C, ultrasonic power 210 W, liquid to solid (L/S) ratio 20 mL/g and n-hexane as the solvent. Meanwhile, 70.21 ± 0.36 % of oil yield was obtained from SE when the extraction time was 240 min, extraction temperature 85 °C, L/S ratio 35 mL/g and n-hexane as the solvent. C. inophyllum seeds oil extracted from these two techniques contained similar types of fatty acids such as oleic acid, palmitic acid, linoleic acid, stearic acid and behenic acid. The UAE process of C. inophyllum seeds oil was further optimized using Response Surface Methodology (RSM) via Box-Behnken design (BBD). The maximum predicted oil yield of 56.20 % was obtained at an extraction time of 21 min, extraction temperature 42 °C, ultrasonic power 210 W, L/S ratio 21 mL/g with n-hexane as the solvent. For the kinetics evaluation of UAE process of C. inophyllum seeds oil, it was found that the Patricelli’s model fitted well to the extraction data with R2 > 0.974 and MRPD value < 10 %. Thus, it is adequate to describe the extraction process of oil from C. inophyllum seeds. 2016-03 Thesis http://eprints.usm.my/45771/ http://eprints.usm.my/45771/1/Extraction%20Of%20Oil%20From%20Calophyllum%20Inophyllum%20Seeds%20Optimization%20And%20Kinetics%20Studies%20Of%20Ultrasonic-Assisted%20Extraction.pdf application/pdf en public masters Universiti Sains Malaysia Pusat Pengajian Kejuruteraan Kimia
institution Universiti Sains Malaysia
collection USM Institutional Repository
language English
topic T Technology
TP155-156 Chemical engineering
spellingShingle T Technology
TP155-156 Chemical engineering
Fuad, Faiznur Mohd
Extraction Of Oil From Calophyllum Inophyllum Seeds Optimization And Kinetics Studies Of Ultrasonic-Assisted Extraction
description Calophyllum inophyllum seeds oil was extracted using two different extraction techniques, namely, ultrasonic-assisted extraction (UAE) and Soxhlet extraction (SE). The highest oil yield attained from UAE was 55.44 ± 0.53 % at an extraction time of 20 min, extraction temperature 40 °C, ultrasonic power 210 W, liquid to solid (L/S) ratio 20 mL/g and n-hexane as the solvent. Meanwhile, 70.21 ± 0.36 % of oil yield was obtained from SE when the extraction time was 240 min, extraction temperature 85 °C, L/S ratio 35 mL/g and n-hexane as the solvent. C. inophyllum seeds oil extracted from these two techniques contained similar types of fatty acids such as oleic acid, palmitic acid, linoleic acid, stearic acid and behenic acid. The UAE process of C. inophyllum seeds oil was further optimized using Response Surface Methodology (RSM) via Box-Behnken design (BBD). The maximum predicted oil yield of 56.20 % was obtained at an extraction time of 21 min, extraction temperature 42 °C, ultrasonic power 210 W, L/S ratio 21 mL/g with n-hexane as the solvent. For the kinetics evaluation of UAE process of C. inophyllum seeds oil, it was found that the Patricelli’s model fitted well to the extraction data with R2 > 0.974 and MRPD value < 10 %. Thus, it is adequate to describe the extraction process of oil from C. inophyllum seeds.
format Thesis
qualification_level Master's degree
author Fuad, Faiznur Mohd
author_facet Fuad, Faiznur Mohd
author_sort Fuad, Faiznur Mohd
title Extraction Of Oil From Calophyllum Inophyllum Seeds Optimization And Kinetics Studies Of Ultrasonic-Assisted Extraction
title_short Extraction Of Oil From Calophyllum Inophyllum Seeds Optimization And Kinetics Studies Of Ultrasonic-Assisted Extraction
title_full Extraction Of Oil From Calophyllum Inophyllum Seeds Optimization And Kinetics Studies Of Ultrasonic-Assisted Extraction
title_fullStr Extraction Of Oil From Calophyllum Inophyllum Seeds Optimization And Kinetics Studies Of Ultrasonic-Assisted Extraction
title_full_unstemmed Extraction Of Oil From Calophyllum Inophyllum Seeds Optimization And Kinetics Studies Of Ultrasonic-Assisted Extraction
title_sort extraction of oil from calophyllum inophyllum seeds optimization and kinetics studies of ultrasonic-assisted extraction
granting_institution Universiti Sains Malaysia
granting_department Pusat Pengajian Kejuruteraan Kimia
publishDate 2016
url http://eprints.usm.my/45771/1/Extraction%20Of%20Oil%20From%20Calophyllum%20Inophyllum%20Seeds%20Optimization%20And%20Kinetics%20Studies%20Of%20Ultrasonic-Assisted%20Extraction.pdf
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