Effect Of Coating Thickness On The Microstructure, Mechanical And Wear Properties Of A1TiN Coatings Deposited Using Arc Ion Plating Technique

AlTiN coatings were deposited on tungsten carbide insert using Al 0.67 TI0.33 cathodes in cathodic arc plating system. The influence of coating layer thickness on the microstructural, mechanical and wear properties of the coatings was investigated. The AlTiN deposition of hard coatings for tooling a...

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Main Author:	Kadhim, Kamil Jawad
Format:	Thesis
Language:	English English
Published:	2016
Subjects:	T Technology (General)
Online Access:	http://eprints.utem.edu.my/id/eprint/18549/1/Effect%20Of%20Coating%20Thickness%20On%20The%20Microstructure%2C%20Mechanical%20And%20Wear%20Properties%20Of%20A1TiN%20Coatings%20Deposited%20Using%20Arc%20Ion%20Plating%20Technique%2024%20Pages.pdf http://eprints.utem.edu.my/id/eprint/18549/2/Effect%20Of%20Coating%20Thickness%20On%20The%20Microstructure%2C%20Mechanical%20And%20Wear%20Properties%20Of%20AlTiN%20Coatings%20Deposited%20Using%20Arc%20Ion%20Plating%20Technique.pdf
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institution	Universiti Teknikal Malaysia Melaka
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language	English English
advisor	Abd Rahman, Md Nizam
topic	T Technology (General) T Technology (General)
spellingShingle	T Technology (General) T Technology (General) Kadhim, Kamil Jawad Effect Of Coating Thickness On The Microstructure, Mechanical And Wear Properties Of A1TiN Coatings Deposited Using Arc Ion Plating Technique
description	AlTiN coatings were deposited on tungsten carbide insert using Al 0.67 TI0.33 cathodes in cathodic arc plating system. The influence of coating layer thickness on the microstructural, mechanical and wear properties of the coatings was investigated. The AlTiN deposition of hard coatings for tooling applications has many advantages. The main drawback of this technique, however, is the formation of macro particles (MPs) during deposition. The deposited AlTiN coating of various thickness was characterized using X-Ray Diffraction (XRD), scanning electron microscopy (SEM), atomic force microscopy (AFM), Rockwell tester, and ball-on-disc machine, to analyze and quantify the following coating properties: grain size, preferred orientation, atomic elements, thickness, micro hardness, adhesion, surface roughness, and coefficient of friction (COF) of the deposited coatings. Base of this study, the increase in layer thickness was closely related to increase in deposition time. The coating thickness had a significant influence on the width of crater wear. The width of crater wear reduced significantly as the coating thickness increased. However beyond 5.815μm, further increment in coating thickness resulted in increase in crater wear width due to presence of larger macro-particles on the coating surface and reduction of coating hardness. The deposited AlTiN coating also showed a strong preferred orientation of (200) and (111) plane for all coating thickness. The values of various surface roughness measured by AFM was at minimum of 0.07157 μm for the coating having thickness of 2.717 μm whereas; the maximum value of Ra was 0.29647 μm for the coating thickness of 8.760 μm. The highest hardness value was 1939.0 HV for coating thickness of 5.815 μm. Based on adhesion slope technique, AlTiN coatings of 3.089 μm thickness had the best adhesion strength. Correlation study indicated that cutting tools crater wear width has the strongest correlation with the coating atomic percentage ratio of Al/Ti, with coefficient of determination R 2 value of 0.7251. The coating hardness and grain size also indicated some correlation with the crater width wear with R2 values of 0.6051 and 0.5184 respectively.
format	Thesis
qualification_name	Doctor of Philosophy (PhD.)
qualification_level	Doctorate
author	Kadhim, Kamil Jawad
author_facet	Kadhim, Kamil Jawad
author_sort	Kadhim, Kamil Jawad
title	Effect Of Coating Thickness On The Microstructure, Mechanical And Wear Properties Of A1TiN Coatings Deposited Using Arc Ion Plating Technique
title_short	Effect Of Coating Thickness On The Microstructure, Mechanical And Wear Properties Of A1TiN Coatings Deposited Using Arc Ion Plating Technique
title_full	Effect Of Coating Thickness On The Microstructure, Mechanical And Wear Properties Of A1TiN Coatings Deposited Using Arc Ion Plating Technique
title_fullStr	Effect Of Coating Thickness On The Microstructure, Mechanical And Wear Properties Of A1TiN Coatings Deposited Using Arc Ion Plating Technique
title_full_unstemmed	Effect Of Coating Thickness On The Microstructure, Mechanical And Wear Properties Of A1TiN Coatings Deposited Using Arc Ion Plating Technique
title_sort	effect of coating thickness on the microstructure, mechanical and wear properties of a1tin coatings deposited using arc ion plating technique
granting_institution	Universiti Teknikal Malaysia Melaka
granting_department	Faculty of Manufacturing Engineering
publishDate	2016
url	http://eprints.utem.edu.my/id/eprint/18549/1/Effect%20Of%20Coating%20Thickness%20On%20The%20Microstructure%2C%20Mechanical%20And%20Wear%20Properties%20Of%20A1TiN%20Coatings%20Deposited%20Using%20Arc%20Ion%20Plating%20Technique%2024%20Pages.pdf http://eprints.utem.edu.my/id/eprint/18549/2/Effect%20Of%20Coating%20Thickness%20On%20The%20Microstructure%2C%20Mechanical%20And%20Wear%20Properties%20Of%20AlTiN%20Coatings%20Deposited%20Using%20Arc%20Ion%20Plating%20Technique.pdf
_version_	1747833934538866688
spelling	my-utem-ep.185492021-10-10T16:29:16Z Effect Of Coating Thickness On The Microstructure, Mechanical And Wear Properties Of A1TiN Coatings Deposited Using Arc Ion Plating Technique 2016 Kadhim, Kamil Jawad T Technology (General) TA Engineering (General). Civil engineering (General) AlTiN coatings were deposited on tungsten carbide insert using Al 0.67 TI0.33 cathodes in cathodic arc plating system. The influence of coating layer thickness on the microstructural, mechanical and wear properties of the coatings was investigated. The AlTiN deposition of hard coatings for tooling applications has many advantages. The main drawback of this technique, however, is the formation of macro particles (MPs) during deposition. The deposited AlTiN coating of various thickness was characterized using X-Ray Diffraction (XRD), scanning electron microscopy (SEM), atomic force microscopy (AFM), Rockwell tester, and ball-on-disc machine, to analyze and quantify the following coating properties: grain size, preferred orientation, atomic elements, thickness, micro hardness, adhesion, surface roughness, and coefficient of friction (COF) of the deposited coatings. Base of this study, the increase in layer thickness was closely related to increase in deposition time. The coating thickness had a significant influence on the width of crater wear. The width of crater wear reduced significantly as the coating thickness increased. However beyond 5.815μm, further increment in coating thickness resulted in increase in crater wear width due to presence of larger macro-particles on the coating surface and reduction of coating hardness. The deposited AlTiN coating also showed a strong preferred orientation of (200) and (111) plane for all coating thickness. The values of various surface roughness measured by AFM was at minimum of 0.07157 μm for the coating having thickness of 2.717 μm whereas; the maximum value of Ra was 0.29647 μm for the coating thickness of 8.760 μm. The highest hardness value was 1939.0 HV for coating thickness of 5.815 μm. Based on adhesion slope technique, AlTiN coatings of 3.089 μm thickness had the best adhesion strength. Correlation study indicated that cutting tools crater wear width has the strongest correlation with the coating atomic percentage ratio of Al/Ti, with coefficient of determination R 2 value of 0.7251. The coating hardness and grain size also indicated some correlation with the crater width wear with R2 values of 0.6051 and 0.5184 respectively. UTeM 2016 Thesis http://eprints.utem.edu.my/id/eprint/18549/ http://eprints.utem.edu.my/id/eprint/18549/1/Effect%20Of%20Coating%20Thickness%20On%20The%20Microstructure%2C%20Mechanical%20And%20Wear%20Properties%20Of%20A1TiN%20Coatings%20Deposited%20Using%20Arc%20Ion%20Plating%20Technique%2024%20Pages.pdf text en public http://eprints.utem.edu.my/id/eprint/18549/2/Effect%20Of%20Coating%20Thickness%20On%20The%20Microstructure%2C%20Mechanical%20And%20Wear%20Properties%20Of%20AlTiN%20Coatings%20Deposited%20Using%20Arc%20Ion%20Plating%20Technique.pdf text en validuser https://plh.utem.edu.my/cgi-bin/koha/opac-detail.pl?biblionumber=101739 phd doctoral Universiti Teknikal Malaysia Melaka Faculty of Manufacturing Engineering Abd Rahman, Md Nizam 1. Abd Rahman, M. N., 2009. Modelling of Physical Vapour Deposition (PVD) Process on Cutting Tool Using Response Surface Methodology ( RSM ). 2. Abu-Shgair, K., Al-Hasan, M., Abdul, J., Al-Bashir, A., Abu-Safe, H.H. and Gordon, M. H., 2010. 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