Influence of alkali resistant (AR) glass in porcelain clay for vitrified clay pipes

The aimed of the present work is to produce porcelain clay reinforced with Alkali Resistant (AR) glass for vitrified clay pipes at minimum sintering temperature. In this study, AR fiberglass as a reinforcement was milled into an average particle size of 90 μm and mixed with porcelain in different we...

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Main Author: Hanapi, Muhammad Ikhmal
Format: Thesis
Language:English
English
English
Published: 2017
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spelling my-uthm-ep.8292021-09-06T02:39:42Z Influence of alkali resistant (AR) glass in porcelain clay for vitrified clay pipes 2017-12 Hanapi, Muhammad Ikhmal TD511-780 Sewage collection and disposal systems. Sewerage The aimed of the present work is to produce porcelain clay reinforced with Alkali Resistant (AR) glass for vitrified clay pipes at minimum sintering temperature. In this study, AR fiberglass as a reinforcement was milled into an average particle size of 90 μm and mixed with porcelain in different weight percentage at 3 wt%, 6 wt%, 9 wt%, and 12 wt%. The sample was prepared by using powder compaction and then fired for 2 hours at 900°C, 1000°C 1100°C and 1200°C. Based on the chemical analysis, it was found that SiO2, Al2O3, Na2O and K2O is the significant element to produce the material. Result of thermal analysis shows that sintering start occurs at 900°C to 1300°C. The result of volume shrinkage, apparent porosity, water absorption, bulk density and flexural strength were recorded for each samples. Scanning electron microscope (SEM) was used to observe the microstructural morphology of samples. It was found that the addition of AR glass can dramatically lowering the apparent porosity as well as water absorption and increase the value of volume shrinkage, bulk density and flexural strength with the rising of sintering temperature. It can be seen that the volume shrinkage is satisfy the typical ceramic shrinkage where is quarter than original dimension which is 31.75%. Based on the result, the favorable properties of porcelain clay sintering were obtained at sintering temperature of 1100°C with addition of 3 wt% AR glass. Thus, the suitable value of apparent porosity, water absorption and density obtained was 0.41%, 6.27% and 2.29g/cm3 respectively. Meanwhile, the maximum value for flexural strength gained was 76.40MPa. Based on the microstructure image, it can be seen that the reduction of porosity and increasing of glassy phase was corresponded to the addition of AR glass and rising of sintering temperature. In conclusion, the objective of this study were achieve to satisfied the value of vitrified clay pipes standard based on EN 295. 2017-12 Thesis http://eprints.uthm.edu.my/829/ http://eprints.uthm.edu.my/829/2/24p%20MUHAMMAD%20IKHMAL%20HANAPI.pdf text en public http://eprints.uthm.edu.my/829/1/MUHAMMAD%20IKHMAL%20HANAPI%20COPYRIGHT%20DECLARATION.pdf text en staffonly http://eprints.uthm.edu.my/829/3/MUHAMMAD%20IKHMAL%20HANAPI%20WATERMARK.pdf text en validuser mphil masters Universiti Tun Hussein Onn Malaysia Fakulti Kejuruteraan Mekanikal dan Pembuatan
institution Universiti Tun Hussein Onn Malaysia
collection UTHM Institutional Repository
language English
English
English
topic TD511-780 Sewage collection and disposal systems
Sewerage
spellingShingle TD511-780 Sewage collection and disposal systems
Sewerage
Hanapi, Muhammad Ikhmal
Influence of alkali resistant (AR) glass in porcelain clay for vitrified clay pipes
description The aimed of the present work is to produce porcelain clay reinforced with Alkali Resistant (AR) glass for vitrified clay pipes at minimum sintering temperature. In this study, AR fiberglass as a reinforcement was milled into an average particle size of 90 μm and mixed with porcelain in different weight percentage at 3 wt%, 6 wt%, 9 wt%, and 12 wt%. The sample was prepared by using powder compaction and then fired for 2 hours at 900°C, 1000°C 1100°C and 1200°C. Based on the chemical analysis, it was found that SiO2, Al2O3, Na2O and K2O is the significant element to produce the material. Result of thermal analysis shows that sintering start occurs at 900°C to 1300°C. The result of volume shrinkage, apparent porosity, water absorption, bulk density and flexural strength were recorded for each samples. Scanning electron microscope (SEM) was used to observe the microstructural morphology of samples. It was found that the addition of AR glass can dramatically lowering the apparent porosity as well as water absorption and increase the value of volume shrinkage, bulk density and flexural strength with the rising of sintering temperature. It can be seen that the volume shrinkage is satisfy the typical ceramic shrinkage where is quarter than original dimension which is 31.75%. Based on the result, the favorable properties of porcelain clay sintering were obtained at sintering temperature of 1100°C with addition of 3 wt% AR glass. Thus, the suitable value of apparent porosity, water absorption and density obtained was 0.41%, 6.27% and 2.29g/cm3 respectively. Meanwhile, the maximum value for flexural strength gained was 76.40MPa. Based on the microstructure image, it can be seen that the reduction of porosity and increasing of glassy phase was corresponded to the addition of AR glass and rising of sintering temperature. In conclusion, the objective of this study were achieve to satisfied the value of vitrified clay pipes standard based on EN 295.
format Thesis
qualification_name Master of Philosophy (M.Phil.)
qualification_level Master's degree
author Hanapi, Muhammad Ikhmal
author_facet Hanapi, Muhammad Ikhmal
author_sort Hanapi, Muhammad Ikhmal
title Influence of alkali resistant (AR) glass in porcelain clay for vitrified clay pipes
title_short Influence of alkali resistant (AR) glass in porcelain clay for vitrified clay pipes
title_full Influence of alkali resistant (AR) glass in porcelain clay for vitrified clay pipes
title_fullStr Influence of alkali resistant (AR) glass in porcelain clay for vitrified clay pipes
title_full_unstemmed Influence of alkali resistant (AR) glass in porcelain clay for vitrified clay pipes
title_sort influence of alkali resistant (ar) glass in porcelain clay for vitrified clay pipes
granting_institution Universiti Tun Hussein Onn Malaysia
granting_department Fakulti Kejuruteraan Mekanikal dan Pembuatan
publishDate 2017
url http://eprints.uthm.edu.my/829/2/24p%20MUHAMMAD%20IKHMAL%20HANAPI.pdf
http://eprints.uthm.edu.my/829/1/MUHAMMAD%20IKHMAL%20HANAPI%20COPYRIGHT%20DECLARATION.pdf
http://eprints.uthm.edu.my/829/3/MUHAMMAD%20IKHMAL%20HANAPI%20WATERMARK.pdf
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