Regenerated cellulose/halloysite nanotube nanocomposite films prepared with an ionic liquid

Novel nanocomposite films based on regenerated cellulose/halloysite nanotube (RC/HNT) have been prepared using an environmentally friendly ionic liquid 1-butyl-3-methylimidazolium chloride (BMIMCl). The structural, morphological, thermal and mechanical properties of the RC/HNT nanocomposites were in...

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主要作者: Mohammad, Soheilmoghaddam
格式: Thesis
出版: 2013
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spelling my-utm-ep.422012020-08-17T02:39:47Z Regenerated cellulose/halloysite nanotube nanocomposite films prepared with an ionic liquid 2013 Mohammad, Soheilmoghaddam TA Engineering (General). Civil engineering (General) Novel nanocomposite films based on regenerated cellulose/halloysite nanotube (RC/HNT) have been prepared using an environmentally friendly ionic liquid 1-butyl-3-methylimidazolium chloride (BMIMCl). The structural, morphological, thermal and mechanical properties of the RC/HNT nanocomposites were investigated using x-ray diffraction (XRD), fourier transform infrared (FTIR), field emission scanning electron microscopy (FESEM), atomic force microscopy (AFM), thermal analysis, and tensile strength measurements. The results obtained revealed interactions between the halloysite nanotubes (HNT) and regenerated cellulose (RC) matrix. The Young’s modulus and tensile strength increased from 1.8 to 4.1 GPa and from 35.30 to 60.50 MPa respectively when 8 wt% (HNT) was incorporated, interestingly without loss of ductility. This indicated higher toughness of the nanocomposites compared to RC. Lower water absorption and higher water contact angle indicated an improved hydrophobicity of RC/HNT nanocomposites compared to RC. The thermal stability and oxygen barrier properties of the nanocomposite films were significantly improved compared with pure RC film. 2013 Thesis http://eprints.utm.my/id/eprint/42201/ http://dms.library.utm.my:8080/vital/access/manager/Repository/vital:76055 masters Universiti Teknologi Malaysia, Faculty of Chemical Engineering Faculty of Chemical Engineering
institution Universiti Teknologi Malaysia
collection UTM Institutional Repository
topic TA Engineering (General)
Civil engineering (General)
spellingShingle TA Engineering (General)
Civil engineering (General)
Mohammad, Soheilmoghaddam
Regenerated cellulose/halloysite nanotube nanocomposite films prepared with an ionic liquid
description Novel nanocomposite films based on regenerated cellulose/halloysite nanotube (RC/HNT) have been prepared using an environmentally friendly ionic liquid 1-butyl-3-methylimidazolium chloride (BMIMCl). The structural, morphological, thermal and mechanical properties of the RC/HNT nanocomposites were investigated using x-ray diffraction (XRD), fourier transform infrared (FTIR), field emission scanning electron microscopy (FESEM), atomic force microscopy (AFM), thermal analysis, and tensile strength measurements. The results obtained revealed interactions between the halloysite nanotubes (HNT) and regenerated cellulose (RC) matrix. The Young’s modulus and tensile strength increased from 1.8 to 4.1 GPa and from 35.30 to 60.50 MPa respectively when 8 wt% (HNT) was incorporated, interestingly without loss of ductility. This indicated higher toughness of the nanocomposites compared to RC. Lower water absorption and higher water contact angle indicated an improved hydrophobicity of RC/HNT nanocomposites compared to RC. The thermal stability and oxygen barrier properties of the nanocomposite films were significantly improved compared with pure RC film.
format Thesis
qualification_level Master's degree
author Mohammad, Soheilmoghaddam
author_facet Mohammad, Soheilmoghaddam
author_sort Mohammad, Soheilmoghaddam
title Regenerated cellulose/halloysite nanotube nanocomposite films prepared with an ionic liquid
title_short Regenerated cellulose/halloysite nanotube nanocomposite films prepared with an ionic liquid
title_full Regenerated cellulose/halloysite nanotube nanocomposite films prepared with an ionic liquid
title_fullStr Regenerated cellulose/halloysite nanotube nanocomposite films prepared with an ionic liquid
title_full_unstemmed Regenerated cellulose/halloysite nanotube nanocomposite films prepared with an ionic liquid
title_sort regenerated cellulose/halloysite nanotube nanocomposite films prepared with an ionic liquid
granting_institution Universiti Teknologi Malaysia, Faculty of Chemical Engineering
granting_department Faculty of Chemical Engineering
publishDate 2013
_version_ 1747816714384441344