Synthesis and characterization of activated carbon from Agarwood (Aquilaria malaccensis) for xenoestrogen treatment

The incidence of water contamination by endocrine-disrupting chemicals (EDCs),xenoestrogen such as bisphenol-A (BPA) and estradiol (EST) is increasing in recentdecades. This study was aimed to synthesize and characterize activate carbon derived fromagarwood (agar AC) for xenoestrogen adsorption. The...

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Main Author:	Sahib, Mosa Jafer
Format:	thesis
Language:	eng
Published:	2020
Subjects:	RM Therapeutics Pharmacology
Online Access:	https://ir.upsi.edu.my/detailsg.php?det=6499
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language	eng
topic	RM Therapeutics Pharmacology
spellingShingle	RM Therapeutics Pharmacology Sahib, Mosa Jafer Synthesis and characterization of activated carbon from Agarwood (Aquilaria malaccensis) for xenoestrogen treatment
description	The incidence of water contamination by endocrine-disrupting chemicals (EDCs),xenoestrogen such as bisphenol-A (BPA) and estradiol (EST) is increasing in recentdecades. This study was aimed to synthesize and characterize activate carbon derived fromagarwood (agar AC) for xenoestrogen adsorption. The synthesis was conducted byphysicochemical activation using sulfuric acid which was employed as an activator at 180oC activation temperature followed by calcination under nitrogen condition. Both BPA andEST were detected in six selected rivers and lakes in Malaysia. Agar AC was characterizedby electron microscopy, X-ray diffraction, micro-Raman, Fourier transform infraredspectroscopy, and Zeta potentials to determine which mechanism produced optimal resultfor the adsorption of BPA and EST. The carbon porosity was determined by nitrogenadsorption-desorption isotherm at 77K using Brunauer-Emmett-Teller (BET) method. Theprepared agar AC was mainly micro and mesoporous in nature with BET surface area 1092m2/g. Optimization results showed an optimum removal of BPA was 86% (at carbon dosage1wt.%, pH 7, contact time of 180 minutes and temperature of 50 C) and EST removal was79% (at pH 11, carbon dosage 4 wt.%). Experimental data were fitted into the Langmuirand Freundlich adsorption isotherm models. Both Langmuir and Freundlich isothermspredicted BPA adsorption of agar AC at R2 values greater than 0.99, signifyingchemisorption and physio-sorption processes. The Freundlich isotherm gives a betteramount of EST uptake onto prepared activated carbon, indicating heterogeneouschemisorption process. In conclusion, the adsorption capacity of prepared agar AC showedhigh adsorption capacity (BPA 439 mg/g, EST 1664 mg/g) compared with the commercialAC. The implication of this study provides green adsorption with high sorption capacitymaterial that can be applied for the removal of BPA and EST from water bodies such asrivers and lakes.
format	thesis
qualification_name
qualification_level	Doctorate
author	Sahib, Mosa Jafer
author_facet	Sahib, Mosa Jafer
author_sort	Sahib, Mosa Jafer
title	Synthesis and characterization of activated carbon from Agarwood (Aquilaria malaccensis) for xenoestrogen treatment
title_short	Synthesis and characterization of activated carbon from Agarwood (Aquilaria malaccensis) for xenoestrogen treatment
title_full	Synthesis and characterization of activated carbon from Agarwood (Aquilaria malaccensis) for xenoestrogen treatment
title_fullStr	Synthesis and characterization of activated carbon from Agarwood (Aquilaria malaccensis) for xenoestrogen treatment
title_full_unstemmed	Synthesis and characterization of activated carbon from Agarwood (Aquilaria malaccensis) for xenoestrogen treatment
title_sort	synthesis and characterization of activated carbon from agarwood (aquilaria malaccensis) for xenoestrogen treatment
granting_institution	Universiti Pendidikan Sultan Idris
granting_department	Fakulti Sains dan Matematik
publishDate	2020
url	https://ir.upsi.edu.my/detailsg.php?det=6499
_version_	1747833269909454848
spelling	oai:ir.upsi.edu.my:64992021-12-07 Synthesis and characterization of activated carbon from Agarwood (Aquilaria malaccensis) for xenoestrogen treatment 2020 Sahib, Mosa Jafer RM Therapeutics. Pharmacology The incidence of water contamination by endocrine-disrupting chemicals (EDCs),xenoestrogen such as bisphenol-A (BPA) and estradiol (EST) is increasing in recentdecades. This study was aimed to synthesize and characterize activate carbon derived fromagarwood (agar AC) for xenoestrogen adsorption. The synthesis was conducted byphysicochemical activation using sulfuric acid which was employed as an activator at 180oC activation temperature followed by calcination under nitrogen condition. Both BPA andEST were detected in six selected rivers and lakes in Malaysia. Agar AC was characterizedby electron microscopy, X-ray diffraction, micro-Raman, Fourier transform infraredspectroscopy, and Zeta potentials to determine which mechanism produced optimal resultfor the adsorption of BPA and EST. The carbon porosity was determined by nitrogenadsorption-desorption isotherm at 77K using Brunauer-Emmett-Teller (BET) method. Theprepared agar AC was mainly micro and mesoporous in nature with BET surface area 1092m2/g. Optimization results showed an optimum removal of BPA was 86% (at carbon dosage1wt.%, pH 7, contact time of 180 minutes and temperature of 50 C) and EST removal was79% (at pH 11, carbon dosage 4 wt.%). Experimental data were fitted into the Langmuirand Freundlich adsorption isotherm models. Both Langmuir and Freundlich isothermspredicted BPA adsorption of agar AC at R2 values greater than 0.99, signifyingchemisorption and physio-sorption processes. The Freundlich isotherm gives a betteramount of EST uptake onto prepared activated carbon, indicating heterogeneouschemisorption process. In conclusion, the adsorption capacity of prepared agar AC showedhigh adsorption capacity (BPA 439 mg/g, EST 1664 mg/g) compared with the commercialAC. The implication of this study provides green adsorption with high sorption capacitymaterial that can be applied for the removal of BPA and EST from water bodies such asrivers and lakes. 2020 thesis https://ir.upsi.edu.my/detailsg.php?det=6499 https://ir.upsi.edu.my/detailsg.php?det=6499 text eng closedAccess Doctoral Universiti Pendidikan Sultan Idris Fakulti Sains dan Matematik Abdulkareem-Alsultan, G., Asikin-Mijan, N., Mansir, N., Lee, H. V., Zainal, Z., Islam, A.,& Taufiq-Yap, Y. H. (2019). Pyro-lytic de-oxygenation of waste cooking oil for green dieselproduction over Ag2O3-La2O3/AC nano-catalyst. 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Synthesis and characterization of activated carbon from Agarwood (Aquilaria malaccensis) for xenoestrogen treatment

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